planarTECH ?????????????????2D?????????????????????????????????????
??2004?????????????????planarTECH ????????????????2D????????????????????????????????????????
??? CVD ????
I. PlanarGROW ???CVD????
planarGROW ?????????????(thermal CVD)????????????????????????????????????????
???????planarGROW-2B, planarGROW-4S??planarGROW-6E ?????????????????????????????????
???
*????????????
planargrow-4S ????
planarGROW ????????????????????????(GUI)??????????????LabVIEW ????????????????
?????????????????????????????????????�???� ??????????????????????????
? ?????????????turbopump ????
Fully Automated PC Control with LabVIEW Front End
User-configurable Auto Process Settings
????????????????
????15?????????????????planarGROW ??????????????????????????????????????
?????? �References�??????????�Installations�?????????????????
?? 2D??CVD ????
II.
PlanarGROW
h-BN CVD ??
planarGROW ??????(h-BN )???????(thermal CVD)??????????????????????2?????(planarGROW-2S
-BN)?????????????????????????????????h-BN?????????(liquid borazine) ??????(solid
ammonia borane)??????????????????(precursor)?????????????(h-BN )????(graphene)??????
PlanarGROW-2S-BN ????
Quartz Tube & Furnace
- Tube Dimensions: 2� (?50*1000mm)
- Heater: Kanthal Wire w/ Glass Wool Molding
- Maximum Temperature: 1,100�C
- Heating Zone: 1-zone, ?100*350mm
- Linear Motion Control Unit
Gas Supply Unit
- Four (4) Celerity TN2900 Mass Flow Controllers
* Hydrogen (H2), 100sccm
* Methane (CH4), 200sccm [For Graphene]
* Argon (Ar): 1,000sccm
* Nitrogen (N2): 1,000sccm
- Source Vapor Feeding System w/ Heating Jacket
- Low Temp. Chiller (-10�C) for Borazine Canister
????????????
?????????
????????????????????????????2D??????????? (BN)???????????planarTECH????????
???????planarGROW-2S-BN ????????????DongGuk??Ki Kang Kim??????????????Ki Kang Kim???????
??????????(BN)?????????planarGROW (???)???????
???? (Growth on Copper)
1. (2013-02-15) Kim, S.M., et al. �Synthesis of Patched or Stacked Graphene and hBN Flakes: A Route to Hybrid Structure Discovery,� Nano Lett., 2013, 13 (3), pp 933�94 | DOI:10.1021/nl303760m
2. (2012-09-12) Kim, K.K., et al. �Synthesis and Characterization of Hexagonal Boron Nitride Film as a Dielectric Layer for Graphene Devices,� ACS Nano, 2012, 6 (10), pp 8583�8590 | DOI:10.1021/nn301675f
3. (2011-11-23) Kim, K.K., et al. �Synthesis of Monolayer Hexagonal Boron Nitride on Cu Foil Using Chemical Vapor Deposition,� Nano Lett., 2012, 12 (1), pp 161�166 | DOI:10.1021/nl203249
???? (Growth on Nickel)
1. (2011-09-02) Shi, Y.M., �Synthesis of Few-Layer Hexagonal Boron Nitride Thin Film by Chemical Vapor Deposition,� Nano Lett., 2010,
10 (10), pp 4134�4139 | DOI:10.1021/nl1023707
III.
PlanarGROW
MoS2 CVD ??
planarGROW???????(MoS2)???????(thermal CVD)?????????????????????????????(MoS2)????
????????????(MoO3)??????????????????????????(SiO2)????????2?????(planarGROW-2S
-MoS2)???????????????????????????????? ?
PlanarGROW-2S-MoS2????
Quartz Tube & Furnace
- Quartz Tube Dimensions: ?50(OD)*1000mm
- Heating Element: Kanthal Wire, Glass Wool Molding
- Maximum Temp: 1,000�C, K-type Thermocouple
- Heating Zone: 2-zones, ?50*300mm Each
- Alumina Tray + Wafer Tray for 10x10mm2 Samples
Gas Supply Unit
- One (1) Celerity TN2900 Mass Flow Controller
* Argon (Ar): 1,000sccm
- Open Mounting Bay for Second (2nd) MFC
????????????